Improved synthesis of monodentate and bidentate 2- and 3-pyridylphosphines |
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| Authors: | Alexander M. Kluwer |
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| Affiliation: | Van’t Hoff Institute for Molecular Sciences, University of Amsterdam, Nieuwe Achtergracht 166, 1018 WV Amsterdam, The Netherlands |
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| Abstract: | Tris(pyridyl)phosphines (2- and 3-pyridyl) and 1,2-bis(di-3-pyridylphosphino)ethane were synthesized in 70-75% yield using a Grignard reagent. The product could be efficiently isolated by solid-liquid extraction with diethylamine. |
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| Keywords: | Synthesis Grignard reaction Pyridylphosphine Monodentate Bidentate 2-Pyridyl 3-Pyridyl |
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