Heterobimetallic diethanolaminate complexes of titanium and zirconium with alkaline earth metals |
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| Authors: | Sharma Kanupriya Sharma Malti Singh Anirudh Mehrotra Ram C. |
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| Affiliation: | (1) Department of Chemistry, University of Rajasthan, Jaipur, 302004, India |
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| Abstract: | Ti(OPri)4 or Zr(OPri)4 · PriOH react with hydrocarbon-insoluble complexes M{(OCH2CH2)NH(CH2CH2OH)}2 (M = Mg, Ca, Sr, Ba) in a 2:1 molar ratio to yield hydrocarbon-soluble heterobimetallic diethanolaminate isopropoxide complexes [M{(OCH2CH2)2NH}2{M (OPri)3}2] (M = Mg, Ca, Sr, Ba; M = Ti, Zr), which have been characterized by elemental analyses, molecular weight measurements and spectroscopic [i.r., n.m.r. (1H and 13C)] studies. |
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