Synthesis of methyl ethers of methyl 2-acetamido-2-deoxy-α-D-glucopyranoside |
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Authors: | E. V. Evtushenko E. Yu. Plisova Yu. S. Ovodov |
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Abstract: | A convenient method is proposed for the synthesis of all the individual methyl ethers of methyl 2-acetamido-2-deoxy-α-D-glucopyranoside based on the partial methylation of 2-acetamido-2-deoxy-α-D-glucopyranoside with dimethyl sulfate in an alkaline medium followed by preparative liquid column chromatography on silica gel of the resulting mixture of methyl ethers. |
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