| 软X射线分光晶体琥珀酸十八酯的生长研究 |
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| 引用本文： | 高绍康,陈建中,庄乃峰,关铁堂. 软X射线分光晶体琥珀酸十八酯的生长研究[J]. 人工晶体学报, 2003, 32(5): 438-441 |
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| 作者姓名： | 高绍康 陈建中 庄乃峰 关铁堂 |
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| 作者单位： | 福州大学化学化工学院,福州,350002;福州大学化学化工学院,福州,350002;福州大学化学化工学院,福州,350002;福州大学化学化工学院,福州,350002 |
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| 基金项目： | 福建省自然科学基金(B92020) |
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| 摘 要： | 本文合成了软X射线分光晶体材料琥珀酸十八酯(OSO),对其样品进行了表征和鉴定.对OSO在多种有机溶剂中的结晶性能进行了研究,结果表明在实验的几种有机溶剂中OSO的成核趋势很强,在甲苯和苯中具有较好的结晶特性.测定了OSO在苯和甲苯中的溶解度曲线,并用溶液降温法进行了晶体生长的实验.
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| 关 键 词： | 琥珀酸十八酯 软X射线 分光晶体 结晶习性 晶体生长 |
| 文章编号： | 1000-985X(2003)05-0438-04 |
| 修稿时间： | 2003-05-26 |
Study on the Growth of Dioctadecyl Succinate Crystals for Soft X-ray Spectroscopy |
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| GAO Shao-kang,CHEN Jian-zhong,ZHUANG Nai-feng,GUAN Tie-tang. Study on the Growth of Dioctadecyl Succinate Crystals for Soft X-ray Spectroscopy[J]. Journal of Synthetic Crystals, 2003, 32(5): 438-441 |
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| Authors: | GAO Shao-kang CHEN Jian-zhong ZHUANG Nai-feng GUAN Tie-tang |
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| Abstract: | Dioctadecyl succinate (OSO) was synthesized by esterification method. The crystal sample was characterized by DSC, XRD and IR spectroscopy. The experimental results of crystallinity in some organic solvents show that there is a strong tendency of spontaneous nucleation in the solution. OSO appears a good crystalline in benzene and toluene. The solubility curves of OSO in both solvents were measured. The crystal growth experiments of OSO were made by the falling temperature method. |
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| Keywords: | dioctadecyl succinate soft x-ray analyzer crystal crystalline habit crystal growth |
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