| 人参中稀有皂苷临界二氧化碳超提取 |
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| 引用本文： | 张乐,宋凤瑞,王琦,刘志强,刘淑莹. 人参中稀有皂苷临界二氧化碳超提取[J]. 应用化学, 2010, 27(12): 1483-1485. DOI: 10.3724/SP.J.1095.2010.00052 |
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| 作者姓名： | 张乐 宋凤瑞 王琦 刘志强 刘淑莹 |
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| 作者单位： | (1.中国科学院长春应用化学研究所 长春 130022；2.吉林农业大学中药材学院 长春) |
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| 基金项目： | 吉林省科技发展重大及重点项目，长春市科技发展项目 |
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| 摘 要： | 针对人参稀有皂苷极性较小的特点，选择超临界二氧化碳流体(SFE-CO2)技术进行提取，最佳提取实验条件为:压力35 MPa,温度50 ℃，夹带剂为70%乙醇，夹带剂用量为1.7 mL/g。 利用高效液相色谱 电喷雾质谱联用分析方法分析其萃取产物，证明该提取方法的提取效率与超声提取接近，且该方法具有环境友好的特点。
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| 关 键 词： | 人参稀有皂苷 超临街二氧化碳流体萃取 高效液相色谱-电喷雾质谱联用分析 |
| 收稿时间： | 2010-01-22 |
| 修稿时间： | 2010-03-03 |
Supercritical CO2 Extracting of Rare Ginsenosides |
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| ZHANG Yue,SONG Feng-Rui,WANG Qi,LIU Zhi-Qiang,LIU Shu-Ying. Supercritical CO2 Extracting of Rare Ginsenosides[J]. Chinese Journal of Applied Chemistry, 2010, 27(12): 1483-1485. DOI: 10.3724/SP.J.1095.2010.00052 |
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| Authors: | ZHANG Yue SONG Feng-Rui WANG Qi LIU Zhi-Qiang LIU Shu-Ying |
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| Affiliation: | (1.Changchun Institute of Applied Chemistry,Chinese Academy of Science,Changchun 130022;2.Faculty of Chinese Medicinal Materials,Jilin Agricultural University,Changchun) |
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| Abstract: | Supercritical CO2 fluid(SFE-CO2) extraction technique was used to extract the rare ginsenosides in processed ginseng, and extracting productions were analyzed by HPLC/ESI-MSn. The optimal extraction conditions were estimated as:the extraction pressure was 35 MPa, the extraction temperature was at 50 ℃， and the concentration of alcohol as entrainer was 70%. The experimental result showed that the extracting efficiency of SFE-CO2 technique is similar with that of transonic extraction. The extracting method using SFE-CO2 technique is in favor of ambient. |
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| Keywords: | rare Ginsenosides supercritical CO2 fluid extraction analyzed by HPLC-ESI-MS |
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