Nd28Fe66B6/Fe50Co50双层纳米复合膜的结构和磁性

利用磁控溅射法制备了Nd₂₈Fe₆₆B₆/Fe_{50Co50 双层纳米复合磁性薄膜，研究了其结构和磁性.经873K退火处理15min 后，利用x射线衍射仪测定薄膜晶体结构，采用俄歇电子能谱仪估算薄膜厚度和超导量子干 涉仪测量其磁性.磁性测量表明，1)该系列薄膜具有垂直于膜面的磁各向异性.从起始磁化曲 线和小回线的形状特征可知，矫顽力机制主要是由畴壁钉扎控制.2)对于固定厚度（10nm） 层的硬磁相Nd-Fe-B和不同厚度（dFeCo=1—100nm）层软磁相FeCo双层纳米复合 膜,剩磁随软磁相FeCo 厚度的增加快速增加，而矫顽力则减少.当dFeCo=5nm 时 ，最大磁能积达到160×１０^３A/m.磁滞回线的单一硬磁相特征说明，硬磁相Nd -Fe-B层和软磁相FeCo层之间的相互作用使两相很好地耦合在一起.剩磁和磁能积的提高是由 于两相磁性交换耦合所致. 关键词： Nd-Fe-B/FeCo双层纳米复合膜 交换耦合 磁性增强}

Preparation and magnetic properties of nanocomposite Nd28Fe66B6 /Fe50Co50 bilayer films

The nanocomposite Nd₂₈Fe₆₆B₆/Fe₅₀Co< sub>50 bilayer films with Mo underlayer and overlayer have been fabricated on Si substrates. All the samples prepared have perpendicular anisotropy and th e hysteresis loops are simple single loops for fixed Nd-Fe-B layer thickness (10 nm) and different FeCo layer thickness (d_FeCo =1—100nm). The shape a nd the behavior of the initial loops and the minor loops suggest that wall pinni ng is the dominant coercivity mechanism in these films. The magnetization of the se samples is found to increase with increasing FeCo layer thickness for a fixed Nd-Fe-B layer thickness and the coercivity of films decrease with increasing Fe Co layer thickness. The sample of maximum energy product is 160×１０^{３A/m for d_FeCo =5nm at room temperature. The enhancement of the rema nence and energy products in nanocomposite bilayer films is attributed to the ex change coupling between the magnetically soft and hard phases.}