Microwave-assisted and conventional synthesis of new phthalocyanines containing 4-(p-fluorophenyl)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one moieties |
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| Authors: | Bahittin Kahveci,Musa Ö zil,Selami ?a?maz,Yavuz Kö ysal |
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| Affiliation: | a Department of Chemistry, Faculty of Art and Science, Rize University, 53050 Rize, Turkey
b Department of Physics, Faculty of Art and Science, Ondokuz May?s University, 55139 Samsun, Turkey |
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| Abstract: | New metal-free and metal (Zn, Ni, Cu and Co) phthalocyanines containing 4-(p-fluorophenyl)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one moiety have been prepared from 1-(3,4-dicyanophenyl)-4-(p-fluorophenyl)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one by both conventional and microwave-assisted methods. All of these compounds are soluble in CHCl3, DMF and DMSO. The new compounds have been characterized by elemental analysis, IR, NMR, UV-Vis spectroscopies. The crystal structures of compounds I and II were also determined by the single crystal diffraction technique. |
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| Keywords: | Microwave Synthesis Phthalocyanine Triazol-5-one |
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