| Synthesis and Crystal Structure of 1′-Methyl-4′- (4-chlorophenyl)-1H-indole-3-spiro-2′-pyrrolidine- 3′-spiro-4'-(2'-phenyloxazole)-2,5'(3H,4'H)-dione |
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| 作者姓名： | 文丽荣 刘鹏 李明 |
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| 作者单位： | College of Chemistry and Molecular Engineering Qingdao University of Science and Technology，College of Chemistry and Molecular Engineering Qingdao University of Science and Technology，College of Chemistry and Molecular Engineering Qingdao University of Science and Technology，Qingdao 266042 China，Qingdao 266042 China，Qingdao 266042 China |
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| 基金项目： | Supported by the National Natural Science Foundation of China (No. 20572057)，Natural Science Foundation of Shandong Province (Y2006B11) |
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| 摘 要： | The title compound (C26H20ClN3O3) has been synthesized by 1,3-dipolar cycloaddition reaction from isatin, sarcosine and (Z)-4-(4-chlorobenzylidene)-2-phenyloxazol-5(4H)-one through a one-pot procedure, and its structure was confirmed by IR, 1H NMR, elemental analysis and single-crystal X-ray diffraction analysis. The crystal belongs to the triclinic system, space group P1, with a = 9.3903(19), b = 11.398(2), c = 12.603(3) , α = 83.495(3), β = 68.988(3), γ = 67.178(3)°, V = 1160.1(4) 3, Z = 2, Mr = 457.90, Dc = 1.311 g/cm3, μ = 0.198 mm-1, F(000) = 476, the final R = 0.0489 and wR = 0.1144 for 3109 observed reflections with I > 2σ(I).
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