Crystal and molecular structure of (2R,3R)-2-exo-((1R)-1-hydroxy-2-methyl-propyl)-3-exo-hydroxymethyl-bicyclo[2.2.1]-hept-5-ene,C12H20O2 |
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| Authors: | A. J. H. Klunder F. J. C. Van Gastel J. M. M. Smits Paul T. Beurskens Gezina Beurskens |
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| Affiliation: | (1) Department of Organic Chemistry, University of Nijmegen, Toernooiveld 1, 6525 ED Nijmegen, The Netherlands;(2) Crystallography Laboratory, University of Nijmegen, Toernooiveld 1, 6525 ED Nijmegen, The Netherlands |
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| Abstract: | The stereogeometry of the title compound which was prepared by a stereoselective addition reaction, has been proved by an X-ray diffraction analysis. Crystal data: monoclinic, P21,a=10.495(16),b=8.392(16),c=13.209(20) Å,  =93.80(8),Z=4. The crystal structure has been solved by vector search methods and refined toR=0.05 for 782 observed reflections. |
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| Keywords: | Mg-chelation controlled asymmetric addition norbornene crystal and molecular structure |
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