One-pot synthesis of tripodal tris(2-aminoethyl)amine derivatives from seven molecular components |
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| Authors: | Ann Almesåker Leone Spiccia Christopher R Strauss |
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| Institution: | a School of Chemistry and ARC Special Research Centre for Green Chemistry, Monash University, Wellington Road, Clayton, Victoria 3800, Australia
b QUILL Centre, The Queen’s University of Belfast, Belfast, Northern Ireland BT9 5AG, United Kingdom |
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| Abstract: | Complex tripodal tris(2-aminoethyl)amine (tren)-based ligands have been prepared in a single-pot reaction of tren with 3 equiv each of cyclohexenone and a benzaldehyde derivative (i.e., from seven components and three molecular types). The highest yield of product was obtained for p-nitrobenzaldehyde, the most electrophilic aldehyde used. |
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