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X-ray structure of tetramethyl thiophenetetracarboxylate
Authors:John N. Bridson  Melbourne J. Schriver  Shuguang Zhu
Affiliation:(1) Department of Chemistry, Memorial University of Newfoundland, A1B 3X7 St. John's, Newfoundland, Canada
Abstract:The X-ray crystal structure of tetramethyl thiophenetetracarboxylate has been determined. Colourless, plates of C12H12O8S crystallise in the orthorhombic space group Pbca with cell dimensionsa=18.321(7),b=17.98(1),c=8.675(6)Å;V=2858(5)Å3 andz=8.1568 unique reflections withInet>2sgr(I) on refinement afforded values ofR=0.040 andRw=0.034.
Keywords:Thiophene  Structure  Carboxylate
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