Crystal structure and spectroscopic characterization of bis(N-phenylthiourea) |
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| Authors: | Narayan T. Akinchan Piotr M. Drożdżewski Luigi P. Battaglia |
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| Affiliation: | (1) Department of Chemistry, University of Calabar, Calabar, Unical Post Box 3619, Nigeria;(2) Institute of Inorganic Chemistry and Metallurgy of Rare Elements, Wroc!["lstrok"]("/content/4rxv83d5463pt4rr/xlarge322.gif") aw University of Technology, Wyb. Wyspianskiego 27, 50-370 Wrocaw, Poland;(3) University of Parma, Viale delle Scienze, 431000 Parma, Italy |
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| Abstract: | Bis(N-phenylthiourea) (BPTU) has been synthesized and characterized by means of X-ray, IR, Raman, UV-Vis, 1H NMR, and FAB mass spectra. The BPTU crystal belongs to the monoclinic C2/c space group with the cell constants a = 26.992(8) Å, b = 6.336(3) Å, c = 9.463(3) Å,  =  = 90°,  = 105.97(7)°, Z = 4. The compound has been found to exist in the thione form, with cis configuration of the thiosemicarbazone moiety and skew conformation of the molecule. |
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| Keywords: | Bis(N-phenylthiourea) crystal structure IR Raman UV-Vis 1H NMR FAB |
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