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Rapid Pretreatment of a Solid Silver Electrode for Routine Analytical Practice
Abstract:A very fast electrochemical method for renovation of solid electrodes and storage of the electrodes in a ready for use state, as well as necessary original hardware, is presented in this work. The device has the shape of a cylindrical container with a volume of about 3–5 mL filled with an electrolyte solution in which auxiliary and reference electrodes are placed. It may be fastened in a typical electrochemical cell. The method relies on suitable electrode polarization in the device. During the renovation process, the electrode is inside the device and immediately after the activation, it is moved into the tested solution where the measurement is realized.
Keywords:Solid electrode  Silver electrode  Electrode pretreatment system  Differential capacity  Voltammetry  Roughness factor
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