Conformational analysis of the -tricyclo[5.1.0.0.3,5] octane ring system: comparison of solution and solid-state geometries |
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Authors: | W Cocker PD Cunningham NWA Geraghty T Higgins PJ McArdle |
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Institution: | Department of Chemistry, Trinity College, Dublin, Ireland.;Department of Chemistry, University College, Galway, Ireland. |
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Abstract: | The six-membered ring of an -tricyclo 5.1.0.0.3,5] octane derivative is shown by X-ray crystallography to be almost planar. The precise conformation agrees remarkably well with that obtained for the molecule in solution using lanthanide shift reagents. |
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