Synthesis and characterization of tetrakis(2,6-diethylphenyl)digermene |
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Authors: | James T. Snow Shu Murakami Satoru Masamune David J. Williams |
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Affiliation: | 1. Department of Chemistry, Massachusetts Institute of Technology Cambridge, Massachusetts 02139, U.S.A.;2. Chemical Crystallography Laboratory, Department of Chemistry Imperial College, London SW7 2AY, U.K. |
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Abstract: | Tetrakis(2,6-diethylphenyl)digermene (1b) has been synthesized and its molecular structure determined: (1) the GeGe bond length is 2.213(2) Å and (2) the molecule has a twist angle of 11° about the GeGe bond and an out-of-plane bending angle of 15° at the germanium atoms. |
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