(endo)-5-(2-haloethyl)-2-norbornene. A new radical probe. |
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Authors: | E.C. Ashby Tung N. Pham |
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Affiliation: | School of Chemistry, Georgia Institute of Technology, Atlanta, GA 30332 USA |
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Abstract: | (endo)-5-(2-haloethyl)-2-norbornenes have been synthesized, and their corresponding radicals generated by reaction with sodium, magnesium, sodium naphthalenide and tri-n-butyltin hydride in the presence of AIBN to produce both straight chain and cyclized products. This probe cyclizes substantially faster than the often used 5-hexenyl halide probes. |
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