Synthesis of 2-oxohexahydrothieno[3,4-d]imidazole derivatives |
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Authors: | S I Zav'yalov O V Dorofeeva |
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Institution: | (1) N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, Moscow |
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Abstract: | Conclusions We synthesized the cis-3- and 4-methyl-2-oxo-6-( -carboxybutyl) hexahydro 3,4-d]-imidazoles by the reduction of the 3- and 4-methyl-2-oxo-2,3-dihydro-6-(carboxybutyl)-1H-thieno 3,4-d] imidazoles with HSiEt3 in CF3COOH and subsequent alkaline hydrolysis of the intermediate methyl ethers.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 7, pp. 1634–1636, July, 1980.The authors express their gratitude to Prof. A. Mark (France) for supplying the sample of 2-oxo-4-methyl-6-(6-carboxybutyl)hexahydrothieno3,4-d]imidazole. |
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