| Crystal Structure of 1，6：3，4－Dianhydro－β－D－galactopyranose－2－O－p－tolylsulfonate（C_13H_14O_6S） |
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| 引用本文： | Wang An-Lai,Lu Shi-Jie,Fu Hong-Xiang,Wang Han-Qing (Lanzhou Institute of Chemical Physics,Chinese Academy of Sciences,Lanzhou,730000)Huang Liang-Ren,Huang Xiao-Ying(Fujian Institute of Research on the Structure of Matter,Chinese Academy of Sciences,Fuz. Crystal Structure of 1，6：3，4－Dianhydro－β－D－galactopyranose－2－O－p－tolylsulfonate（C_13H_14O_6S）[J]. 结构化学, 1996, 0(4) |
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| 作者姓名： | Wang An-Lai Lu Shi-Jie Fu Hong-Xiang Wang Han-Qing (Lanzhou Institute of Chemical Physics Chinese Academy of Sciences Lanzhou 730000)Huang Liang-Ren Huang Xiao-Ying(Fujian Institute of Research on the Structure of Matter Chinese Academy of Sciences Fuz |
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| 作者单位： | Wang An-Lai;Lu Shi-Jie;Fu Hong-Xiang;Wang Han-Qing (Lanzhou Institute of Chemical Physics，Chinese Academy of Sciences，Lanzhou，730000 |
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| 摘 要： | ＣｒｙｓｔａｌＳｔｒｕｃｔｕｒｅｏｆ１，６：３，４－Ｄｉａｎｈｙｄｒｏ－β－Ｄ－ｇａｌａｃｔｏｐｙｒａｎｏｓｅ－２－Ｏ－ｐ－ｔｏｌｙｌｓｕｌｆｏｎａｔｅ（Ｃ_１３Ｈ_１４Ｏ_６Ｓ）ＷａｎｇＡｎ－Ｌａｉ；ＬｕＳｈｉ－Ｊｉｅ；ＦｕＨｏｎｇ－Ｘｉａｎｇ；Ｗａ?..
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Crystal Structure of 1 ,6 : 3, 4-Dianhydro-β-D-galactopyranose-2-O-p-tolylsulfonate(C_13H_14O_6S) |
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| Wang An-Lai,Lu Shi-Jie,Fu Hong-Xiang,Wang Han-Qing. Crystal Structure of 1 ,6 : 3, 4-Dianhydro-β-D-galactopyranose-2-O-p-tolylsulfonate(C_13H_14O_6S)[J]. Chinese Journal of Structural Chemistry, 1996, 0(4) |
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| Authors: | Wang An-Lai Lu Shi-Jie Fu Hong-Xiang Wang Han-Qing |
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| Abstract: | A dianhydro sugar derivative, (C_13H)14O_6S), M_r=298. 3. Orthorhombic P2_12_12_1, a=6. 28(1), b=13. 467(4), c=15.751 (2) A, V=1319. 0(5)A￣3, μ( MoKα)=2. 56cm￣(-1), D_c=1. 50 g/cm￣3, Z=4, F(000)=624, final R=0. 041, R_w=0. 050 for 1488 observed reflections. The pyranose ring in the dianhydro sugar appears a half-chair conformation owing to the effect of 3, 4-oxirane ring. |
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| Keywords: | dianhydro sugar synthesis crystal structure |
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