Reaction of ethynylsilanes with perfluoroiodoalkanes |
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Authors: | M G Voronkov O G Yarosh L N Il'icheva |
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Institution: | (1) Irkutsk Institute of Organic Chemistry, Siberian Branch, Academy of Sciences of the USSR, USSR |
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Abstract: | Conclusion The addition of iodotrifluoromethane, 1-iodoperfluoropropane, and 1-iodo-1,1,2,2,3,3,4,4-octafluorobutane to alkylethynyl- and alkylalkoxyethynylsilanes gave the 1-iodo-3,3,3-trifluoropropen-1-ylsilanes, 1-iodo-3,3,3,4,5-5,5-heptafluoropenten-1-ylsilanes, and 1-iodo-3,3,4,4,5,5,6,6-octafluorohexen-1-ylsilane. The corresponding fluorosilanes were synthesized by reacting the latter with 40% aqueous HF solution.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 6, pp. 1424–1428, June, 1982. |
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