Determination of petroleum trace impurities in aqueous samples by chromatography in a steam flow |
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Authors: | A V Chuikin S V Grigor’ev A A Velikov |
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Institution: | (1) Institute of Petrochemistry, Siberian Division, Russian Academy of Sciences, Akademicheskii pr. 3, Tomsk, 634021, Russia |
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Abstract: | A procedure was developed for the determination of trace petroleum products in water by gas chromatography with steam as the carrier gas. Solid-phase microextraction was used for sample preparation. A method for the stabilization and homogenization of water samples before the analysis and a method for the removal of polar components of the sample were proposed. The precision and accuracy indices of the proposed procedure were estimated for aqueous solutions of a mixture of diesel fuel and oil with a concentration close to the maximum permissible concentration. The relative error in the measurement is no more than ~25% in the concentration range of petroleum products of 0.05–0.5 mg/L. |
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