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Synthesis and crystal structure of ethyl 1-benzyl-2-hydroxy-5-methyl-3-oxo-2-phenacyl-2,3-dihydropyrrole-4-carboxylate
Authors:Z. G. Aliev  S. N. Shurov  E. Yu. Pavlova  Yu. S. Andreichikov  L. O. Atovmyan
Affiliation:(1) Institute of Chemical Physics in Chernogolovka, Russian Academy of Sciences, 142432 Chernogolovka, Moscow Region, Russian Federation;(2) Perm' State University, 15 ul. Bukireva, 614600 Perm', Russian Federation;(3) Institute of Technical Chemistry, Ural Branch of the Russian Academy of Sciences, 13 ul. Lenina, 614600 Perm', Russian Federation
Abstract:Reaction of 5-phenyl-2,3-dihydro-2,3-furandione with ethyl 3-benzylamino-2-butenoate, resulting in ethyl 1-benzyl-2-hydroxy-5-methyl-3-oxo-2-phenacyl-2,3-dihydropyrrole-4-carboxylate and benzylamide ofN-benzoylpyruvic acid, was studied. The structure of the pyrrole derivative was confirmed by X-ray analysis.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 8, pp. 1552–1555, August, 1995.
Keywords:5-phenyl-2,3-dihydro-2,3-furandione  ethyl 3-benzylamino-2-butenoate  ethyl 1-benzyl-2-hydroxy-5-methyl-3-oxo-2-phenacyl-2,3-dihydropyrrole-4-carboxylate  crystal and molecular structure
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