The Effect of Preparation Method and Calcination Temperature on the Crystallite Size and Surface Area of Perovskite-Type SrFeO x |
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Authors: | Abdul Majid Jim Tunney Steve Argue Mike Post |
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Affiliation: | (1) Institute for Chemical Process and Environmental Technology, National Research Council of Canada, Ottawa, Ontario, K1A 0R9, Canada |
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Abstract: | We have investigated the synthesis of perovskite-type SrFeOx (2.5 x 3.0) using three preparative methods: sol-gel, mechanochemical processing and solid state reactions at high temperature of the corresponding oxides. The sample obtained after calcination of the gel from sol-gel method, contained the least amount of strontium carbonate impurity. The amount of strontium carbonate impurity decreased with the increase in calcination temperature. Perovskites obtained have been characterized by X-ray diffraction (XRD) and nitrogen adsorption isotherms. Samples obtained from three methods have been compared with respect to calcination temperature, crystallite size and specific surface area.Issued as NRCC No. 46479. |
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Keywords: | mechanochemical processing perovskites sol-gel SrFeOx |
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