| 微波溶样—电感耦合等离子体光谱法测定粗氧锑中Hg和As |
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| 引用本文： | 钟莹 何慧. 微波溶样—电感耦合等离子体光谱法测定粗氧锑中Hg和As[J]. 光谱学与光谱分析, 2000, 20(2): 232-236 |
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| 作者姓名： | 钟莹 何慧 |
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| 作者单位： | 深圳出入境检验检疫局!518045深圳 |
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| 摘 要： | 本文采用盐酸 酒石酸 氯化钾微波消解样品 ,ICP AES法连续测定粗氧锑中Hg和As的含量。测定粗氧锑的相对偏差 (RSD) :Hg为 0 87%～ 3 2 % ,As为 1 3%～ 2 9% ;回收率 :90 %～ 10 7%
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| 关 键 词： | 粗氧锑 ICP－AES 砷 汞 测定 氧化锑 |
Determination of Hg and As in Crude Antimony Trioxide by Microwave Process System and ICP-AES |
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| Ying ZHONG,Hui HE and Qingbo ZHANG Shenzhen Entry Exit Inspection and Quarntine Bureau, Shenzhen. Determination of Hg and As in Crude Antimony Trioxide by Microwave Process System and ICP-AES[J]. Spectroscopy and Spectral Analysis, 2000, 20(2): 232-236 |
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| Authors: | Ying ZHONG Hui HE Qingbo ZHANG Shenzhen Entry Exit Inspection Quarntine Bureau Shenzhen |
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| Affiliation: | Shenzhen Entry-Exit Inspection and Quarntine Bureau, 518045 Shenzhen. |
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| Abstract: | An ICP-AES method was established for the simultaneous determination of Hg and As in crude antimony trioxide. The samples with different grades were digested in hydrochloric acid-tartraic acid-potassium chloride using microwave process system. The method is applied to analyze crude antimony trioxide with RSD% of 0.87%-3.2% for Hg, 1.3%-2.9% for As, and recovery of 90%-107% |
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| Keywords: | Crude antimony trioxide Microwave process system ICP AES |
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