Hydroxy(tosyloxy)iodo]benzene mediated alpha-azidation of ketones |
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| Authors: | Prakash Om Pannu Kamaljeet Prakash Richa Batra Anita |
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| Affiliation: | Department of Chemistry, Kurukshetra University, Kurukshetra, Haryana, India. dromprakash50@rediffmail.com |
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| Abstract: | Reaction of various ketones with [hydroxy(tosyloxy)iodo]benzene (HTIB) followed by treatment of the alpha-tosyloxy ketones thus generated in situ with NaN3 offers a one-pot procedure for the synthesis of alpha-azido ketones. The HTIB used in this conversion may also be generated in situ by using iodosobenzene in combination with p-toluene-sulphonic acid. |
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