REACTIONS OF TETRAPHOSPHORUS DECASULFIDE AND LAWESSON'S REAGENT WITH SILANES CONTAINING A FEW Si-O BONDS |
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| Authors: | Il'yas S. Nizamov Alexey E. Popovich Elvira S. Batyeva Nail M. Azancheev Vladimir A. Al'fonsov |
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| Affiliation: | A. E. Arbuzov Institute of Organic and Physical Chemistry, Russian Academy of Sciences , Arbuzov Sir, 8, 420088 , Kazan , Russia |
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| Abstract: | Abstract The reactions of tetraphosphorus decasulfide and Lawesson's reagent with tetra-, tri- and dialkoxysilanes were studied. On the basis of these reactions, new S-silyl esters of phosphorus(V) thioacids have been prepared. The prepared compounds were identified by IR, 1H, and 31P NMR and mass spectra as well as elemental analyses. |
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| Keywords: | Tetraphosphorus decasulfide Lawesson's reagent silanes organothiophosphorus compounds |
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