Synthesis and Characterization of O,O-Dimethyl-N-(2,2,2-trichloro-1-arylaminoethyl) Phosphoramidothioates |
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| Authors: | Baolei Wang Xinghai Liu Zhengming Li |
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| Affiliation: | Elemento-Organic Chemistry Institute, State-Key Laboratory of Elemento-Organic Chemistry , Nankai University , Tianjin, China |
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| Abstract: | Several novel trichloromethyl-containing O,O-dimethyl phosphoramidothioate derivatives have been synthesized by the reaction of O,O-dimethyl phosphoramidothioate with chloral imines. The latter were prepared in good yields by refluxing the dichloroethane solution of chloral and substituted anilines using 3 Å molecular sieves as dehydrating agent. Structures of title compounds were confirmed by IR, 1H NMR, 31P NMR, and FT-MS studies. |
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| Keywords: | Phosphoramidothioate synthesis trichloromethyl |
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