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An Efficient,Basic Resin-Mediated,One-Pot Synthesis of Dithiocarbazates Through Alcoholic Tosylates
Authors:Devdutt Chaturvedi  Nisha Mishra  Amit K Chaturvdi  Virendra Mishra
Institution:1. Bio-Organic Chemistry Division , Indian Institute of Integrative Medicine , Jammu-Tawi, J. &2. K, India;3. Synthetic Research Laboratory, Department of Chemistry , B. S. A. College , Mathura, U. P., India
Abstract:A quick and efficient, one-pot synthesis of dithiocarbazates was accomplished in high yields by the reaction of various alcoholic tosylates of primary, secondary, and tertiary alcohols, with substituted hydrazines using an Amberlite IRA 400 (basic resin)/CS 2 system. The reaction conditions are mild with simpler work-up procedures than previously reported methods.
Keywords:Alcoholic tosylates  Amberlite IRA 400  carbon disulfide  dithiocarbazates  substituted hydrazines
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