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SYNTHESIS OF 1-(O,O-DIALKYLPHOSPHORYLAMIDO)PROPYL-5-AZA-2,8,9-TRIOXA-1 SILATRICYCLO-[3,3,3,01,5] UNDECANES
Authors:Zhonghua Li  Xiuyan Song
Affiliation:Central China Normal University , Wuhan, China
Abstract:Ten 1-(O,O-dialkyl phosphorylamido)propyl-5-aza-2,8,9-trioxa-1-silatricyclo [3,3,3,01,5] undecanes were synthesized by the reaction of dialkoxy phosphoryl chlorides with aminopropyl silatrane and their structures were established by elemental analysis, IR, 1HNMR, and MS measurement. The suitable reaction conditions are discussed based on the related reaction mechanism.
Keywords:Organosilicon compound  phosphoroamide  silatrane
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