Abstract: | The reaction in 1:1 molar ratio of {\gg4}OGOAsCl , where G = CH 2 CH 2 , CHMeCHMe, CMe 2 CMe 2 , CHMeCH 2 CMe 2 , and CMe 2 CH 2 CH 2 CMe 2 , and substituted phenols ArOH (Ar = C 6 H 3 Me 2 -2,6; C 6 H 3 Pr i -5-Me-2; C 6 H 3 Pr i -2-Me-5 and C 6 H 3 Pr i 2 -2,6), in the presence of one equivalent of triethylamine in benzene afford volatile colorless liquids of the type {\gg4}OGOAsOAr . All these derivatives have been characterized by elemental analyses, molecular weight measurements, and spectroscopic IR, NMR( 1 H and 13 C)] studies. |