Convenient and Highly Efficient Inversion of 1β-OH Configuration of trans-Vitamin D3 |
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作者姓名: | Yong Bin HAN Jin Ping CHEN Ying Ying LI Bai Ning LIU Guo Qiang YANG Yi LI |
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作者单位: | [1]Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100101 [2]Key Laboratory of Photochemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080 [3]Graduate School, Chinese Academy of Sciences, Beijing 100039 |
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基金项目: | We are greatly grateful to the Major State Basic Research Development Program, Grant No. F2000078100, the National Natural Science Foundation of China (No.20172059) and Chinese Academy of Sciences. |
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摘 要: | A convenient and highly efficient conversion of 1β-OH-trans-vitamin D3, a main byproduct in synthesis of active vitamin D3, to 1α-OH-trans-vitamin D3 is reported. The conversion could be accomplished in 1 minute with 90% yield.
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关 键 词: | 维他命 维生素 生物活性 合成方法 反应条件 |
收稿时间: | 2005-01-31 |
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