| One-Pot Method for Synthesis of Calix[6]biscrowns |
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| 作者姓名： | GUAN Bing
LU Xue-Ran
WU Xiao-Jun
CHEN Yuan-Yin |
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| 作者单位： | GUAN,Bing（Department of Chemistry, Wuhan University, Wuhan 430072）
LU,Xue-Ran（Department of Chemistry, Wuhan University, Wuhan 430072）
WU,Xiao-Jun（Department of Chemistry, Wuhan University, Wuhan 430072）
CHEN,Yuan-Yin（Department of Chemistry, Wuhan University, Wuhan 430072） |
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| 摘 要： | p-tert-Butylcalix6]-1,4-2,5-biscrown-4 is a typical member of the family of calix6]crowns. In the literature, the compound was synthesized from calix6]arene by two steps and the overall yield based on calix6]arene was 24%.Herein we wish to report a one-pot method to do this work. By this method the yield was up to 48% and the reaction time was greatly reduced.
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One-Pot Method for Synthesis of Calix[6]biscrowns |
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| GUAN,Bing,LU,Xue-Ran,WU,Xiao-Jun,CHEN,Yuan-Yin.One-Pot Method for Synthesis of Calix[6]biscrowns[J].Chinese Journal of Organic Chemistry,2004,24(Z1):283. |
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| Authors: | GUAN Bing LU Xue-Ran WU Xiao-Jun CHEN Yuan-Yin |
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| Abstract: | p-tert-Butylcalix6]-1,4-2,5-biscrown-4 is a typical member of the family of calix6]crowns. In the literature, the compound was synthesized from calix6]arene by two steps and the overall yield based on calix6]arene was 24%.Herein we wish to report a one-pot method to do this work. By this method the yield was up to 48% and the reaction time was greatly reduced. |
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