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总磷测定仪校准方法
引用本文:吴永顺,黄金梅,李域,于得水. 总磷测定仪校准方法[J]. 化学分析计量, 2021, 30(1): 72-75
作者姓名:吴永顺  黄金梅  李域  于得水
作者单位:陕西省计量科学研究院,西安 710065;陕西省计量科学研究院,西安 710065;陕西省计量科学研究院,西安 710065;陕西省计量科学研究院,西安 710065
摘    要:建立总磷测定仪的校准方法。介绍了总磷测定仪的工作原理。总磷测定仪的校准包括温度示值误差和温场均匀性、消解时间示值误差、仪器示值误差、测量重复性、示值稳定性5个项目。利用实验数据确定了总磷测定仪的技术指标:温度示值误差不超过±2℃,温场均匀性不大于3℃,消解时间示值误差为不超过±2%,仪器示值误差为不超过±10%,仪器重复性为不大于5%,示值稳定性为不超过±8%FS。该方法可用于总磷测定仪的校准,保证测量数据的准确可靠。

关 键 词:总磷测定仪  校准方法  计量性能

Calibration method of total phosphorus analyzer
Wu Yongshun,Huang Jinmei,Li Yu,Yu Deshui. Calibration method of total phosphorus analyzer[J]. Chemical Analysis And Meterage, 2021, 30(1): 72-75
Authors:Wu Yongshun  Huang Jinmei  Li Yu  Yu Deshui
Affiliation:(Shanxi Institute of Metrology Science,Xi'an 710065,China)
Abstract:The calibration method of total phosphorus analyzer was established.The working principle of total phosphorus analyzer was introduced.The calibration included five items:temperature indication error and temperature field uniformity,digestion time indication error,instrument indication error,instrument repeatability and indication stability.Based on the experimental data,the technical indexes of the total phosphorus analyzer were determined:the temperature indication error was not more than±2℃,the temperature field uniformity was not more than 3℃,the digestion time indication error was not more than±2%,the instrument indication error was not more than±10%,the instrument repeatability was not more than 5%,and the indication stability was not more than±8%FS.This method can be used to calibrate the total phosphorus analyzer to ensure the accuracy and reliability of the measured data.
Keywords:total phosphorus analyzer  calibration method  metrological performance
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