| 无溶剂微波辐射合成双缩二氨基硫脲类化合物 |
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| 引用本文： | 白银娟,路军,杨玲,师蔚鹏,史真. 无溶剂微波辐射合成双缩二氨基硫脲类化合物[J]. 有机化学, 2004, 24(11): 1472-1474 |
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| 作者姓名： | 白银娟 路军 杨玲 师蔚鹏 史真 |
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| 作者单位： | 1. 西北大学化学系,西安,710069
2. 西北大学化学系,西安,710069;新疆塔里木农垦大学文理学院,阿拉尔,84300 |
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| 摘 要： | 在无催化剂无溶剂微波辐射下用芳香醛和1,3-二氨基硫脲合成了双缩二氨基硫脲类化合物,为该类化合物提供了一种新的简便合成方法.产物结构经1H NMR和IR得到确证.
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| 关 键 词： | 无溶剂 微波辐射 1 3-二氨基硫脲 芳香醛 双缩二氨基硫脲 |
| 修稿时间： | 2004-03-16 |
Microwave-Enhanced Synthesis of Thiocarbonohydrazones under Solvent-Free Conditions |
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| BAI,Yin-Juan,a LU,Jun a YANG,Ling a,b SHI,Wei-Peng a SHI,Zhen a. Microwave-Enhanced Synthesis of Thiocarbonohydrazones under Solvent-Free Conditions[J]. Chinese Journal of Organic Chemistry, 2004, 24(11): 1472-1474 |
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| Authors: | BAI Yin-Juan a LU Jun a YANG Ling a b SHI Wei-Peng a SHI Zhen a |
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| Abstract: | The microwave-enhanced synthesis of thiocarbonohydrazones from aromatic aldehydes and thiocarbonohydrazide under solvent-free conditions without catalyst was achieved. This method is a good option to obtain the title compounds in a simple and inexpensive way. Their structures were confirmed by 1H NMR and IR spectra. |
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| Keywords: | solvent-free microwave irradiation thiocarbonohydrazide aromatic aldehyde thiocarbonohydrazone |
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