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Growth and characterization of organic material 4-nitrobenzaldehyde single crystal using modified vertical Bridgman technique
Authors:T Suthan  NP Rajesh
Institution:Centre for Crystal Growth, SSN College of Engineering, Kalavakkam-603110, India
Abstract:The organic material 4-nitrobenzaldehyde single crystal has been grown using the single wall ampoule with nano-translation by modified vertical Bridgman technique. The grown crystal was confirmed by single and powder X-ray diffraction (XRD). Fourier transform infrared (FTIR) analysis was used to identify the functional groups present in the grown crystal. The optical property of the grown crystal was analyzed by UV–vis–NIR and photoluminescence (PL) spectral measurements. The thermal characteristics of the grown crystal were analyzed by thermogravimetric (TG) and differential thermal analyses (DTA). The dielectric measurements were carried out with four different frequencies and the results indicate an increase in dielectric and conductivity parameters with the increase of temperature at all frequencies. The microhardness measurements were used to analyze the mechanical property of the grown crystal.
Keywords:A1  X-ray diffraction  A2  Bridgman technique  A2  Single crystal growth  B1  Organic compounds  B2  Dielectric materials
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