Crystal Structure of 4,7-Dichloro-1,2,3,5,6,8-hexakis-(4-methoxy-phenylsulfanyl)-acenaphthylene |
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| Authors: | Shun-Liu Deng Sa Li Rong-Bin Huang Lan-Sun Zheng |
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| Institution: | (1) Department of Chemistry, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen, Fujian, 361005, P.R. China;(2) The Key Laboratory for Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen, Fujian, 361005, P.R. China |
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| Abstract: | Abstract The title compound was prepared from the reaction of perchloroacenaphthylene with an excess of sodium salt of 4-methyloxythiophenol
in toluene/ethanol (1:1) solvent and structurally characterized by single-crystal X-ray diffraction. The compound crystallizes
in the Monoclinic space group P2(1) with the parameters: a = 10.351(1) ?, b = 20.453(3) ?, c = 12.1837(16) ?, β = 105.584(3)°, V = 2484.5(6) ?3, with Z = 2 formula units.
Graphical Abstract
The title compound 4,7-dichloro-1,2,3,5,6,8-hexakis-(4-methoxy-phenylsulfanyl)-acenaphthylene was synthesized from perchloroacenaphthylene C
12
Cl
8
with an excess of 4-methoxybenzene thiolate in toluene/ethanol (1:1)
 . |
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| Keywords: | Acenaphthylene X-ray crystallography C– H···O interaction |
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