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气相色谱法测定水中的松节油
引用本文:孙欣阳,梁柱,陈晓娟.气相色谱法测定水中的松节油[J].化学分析计量,2009,18(1).
作者姓名:孙欣阳  梁柱  陈晓娟
作者单位:1. 苏州市环境监测中心站,苏州,215004
2. 苏州市环境科学研究所,苏州,215004
摘    要:研究了测定水中松节油的气相色谱法.采用二硫化碳萃取,DB-5型毛细管柱分离,氢火焰检测器(FID)检测水中松节油的含量.松节油浓度在1. 00~25. 0 mg/L范围内与色谱峰面积呈良好的线性关系,线性相关系数r=0. 9996.加标回收率为86. 3%~91. 3%,测定结果的相对标准偏差为8. 7%(n=6).该法可满足地表水环境质量标准的要求.

关 键 词:松节油  气相色谱法  

DETERMINATION OF TURPENITINE IN WATER BY GAS CHROMATOGRAPHY
Sun Xinyang,Liang Zhu,Chen Xiaojuan.DETERMINATION OF TURPENITINE IN WATER BY GAS CHROMATOGRAPHY[J].Chemical Analysis And Meterage,2009,18(1).
Authors:Sun Xinyang  Liang Zhu  Chen Xiaojuan
Institution:Suzhou Environmental Science Monitoring Center;Suzhou 215004;China;Suzhou Environmental Science Research Institute;China
Abstract:Turpentine in water was detected by gas chromatography method,which separated with type of DB-5 column,detected by FID detector.Turpentine concentration was linear with the peak area in the range of 1.00-25.0 mg/L.The recoveries of turpentine were 86.3%-91.3%,and the RSD of determination results was 8.7%(n=6).This method could meet the requirement of GB 3838-2002.
Keywords:gas chromatography  turpentine  water  
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