High-resolution 1H NMR spectroscopy in the solid state: very fast sample rotation and multiple-quantum coherences |
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Authors: | Schnell I Spiess H W |
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Affiliation: | Max-Planck-Institut für Polymerforschung, Postfach 3148, Mainz, D-55021, Germany. schnelli@mpip-mainz.mpg.de |
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Abstract: | In the past few years, solid-state 1H NMR spectroscopy under fast magic-angle spinning (MAS) has developed into a versatile tool for elucidating structure and dynamics. Dipolar multiple-quantum (MQ), in particular double-quantum (DQ), MAS spectroscopy has been applied to a variety of materials and provided unique insight, e.g., into the structure of hydrogen-bonded systems. This review intends to present solid-state 1H DQ and MQ MAS spectroscopy in a systematic fashion with a particular emphasis on methodological aspects, followed by an overview of applications. |
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