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A compact TOF-SANS using focusing lens and very cold neutrons
Authors:Masako Yamada  Yoshihisa IwashitaToshiji Kanaya  Norifumi L. YamadaHirohiko M. Shimizu  Kenji MishimaMasahiro Hino  Masaaki KitaguchiKatsuya Hirota  Peter GeltenbortBruno Guerard  Giuliana ManzinKen Andersen  Jyotsana LalJohn M. Carpenter  Markus BleuelShane J. Kennedy
Affiliation:a ICR, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan
b KEK, 1-1 Oho, Tsukuba, Ibaraki 305-0801, Japan
c KURRI, 2-1010 Kumatori, Osaka 590-0494 Japan
d RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198, Japan
e Institut Laue-Langevin, 6 Rue Jules Horowitz, B.P.156, F-38042 Grenoble Cedex 9, France
f Biosciences Division, ANL, IL 60439, USA
g APS Engineering Support Division, ANL, IL 60439, USA
h Reactor Institut Delft TU, Mekelweg 15, 2629 JB Delft, The Netherlands
i Bragg Institute, ANSTO, Lucas Heights, NSW 2234, Australia
Abstract:We are developing a high-resolution small angle neutron scattering instrument for very cold neutrons (VCN). Our concept includes a magnetic lens for focusing of the beam at the detector plane. The lens consists of one permanent-magnet sextupole array rotating outside another stationary sextupole array, to focus a pulsed white beam of neutrons. Thus the instrument operates in time of flight mode. The prototype magnetic lens has a bore of 15 mm diameter and length of 66 mm, producing a magnetic field gradient oscillating from 1.5×104 to 5.9×104 T/m2, with frequency ≤25 Hz. A torque-canceling magnet around the lens suppresses the torque of rotation from the outer array to 1/3.We have demonstrated the performance of the lens, over wavelength range from 30 to 48 Å, on the PF2-VCN beam line at the Institut Laue-Langevin, France. The focused beam image was the same size as the source, without chromatic aberration, with focal length of 1.14 m. We also studied the performance of this configuration for high-resolution SANS, in a compact geometry (just 5 m long). The measurable q range of this system was 0.009 Å−1q≤0.3 Å−1 or 0.004 Å−1q≤0.08 Å−1 for sample to detector distances of 100 and 465 mm, respectively. Here, we present the results of our lens characterization study along with the SANS results on a tri-block copolymer (F127 Pluronic) and on a stretched polymer blend (with the Shish-Kebab structure).
Keywords:Focusing lens   Rot-PMSx   Pulsed neutron beams   TOF   High resolution   Compact instrument   VCN   Focusing-SANS
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