Synthesis of cyclic sulfides |
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Authors: | V I Dronov V P Krivonogov |
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Institution: | (1) Institute of Chemistry, Bashkirskii Branch, Academy of Sciences of the USSR, Ufa |
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Abstract: | 2,8-Dimethyl-1-thiahydrindan and 9-methyl-1-thiadecalin, respectively, were obtained by the reaction of 1-methyl-1-cyclohexene episulfide with allylmagnesium bromide and subsequent intramolecular cyclization of the resulting 1-methyl-2-allylcyclohexane-1-thiol by the action of sulfuric acid or UV irradiation. The cyclization proceeds stereospecifically.See 1] for communication V.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 9, pp. 1186–1188, September, 1972. |
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