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Substituted phenylarsonic acids; structures and spectroscopy
Authors:Nicholas C. Lloyd  Ron S. Ronimus
Affiliation:School of Science and Engineering, University of Waikato, Private Bag 3105, Hamilton 3240, New Zealand
Abstract:Full NMR and ESI-MS spectra, and differential scanning calorimeter data are presented for 15 substituted phenylarsonic acids, including two new fluoro-substituted examples. X-ray crystal structure determinations of five examples (phenylarsonic acid and the 4-fluoro-, 4-fluoro-3-nitro-, 3-amino-4-hydroxy- and 3-amino-4-methoxy-substituted derivatives) were determined and the H-bonding crystal-packing patterns analysed.
Keywords:Phenyl arsonic acid   Crystal structure   Hydrogen-bonding   NMR spectra
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