| ICP-MS法测定彭泽贝母中微量元素的含量及形态分析 |
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| 引用本文： | 衷友泉,杨婕,韩修林,曹岚,万春花.ICP-MS法测定彭泽贝母中微量元素的含量及形态分析[J].分析测试技术与仪器,2006,12(4):208-212. |
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| 作者姓名： | 衷友泉 杨婕 韩修林 曹岚 万春花 |
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| 作者单位： | 1. 江西中医学院,江西,南昌,330006
2. 江西省分析测试中心,江西,南昌,330029 |
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| 基金项目： | 国家自然科学基金;江西省科技厅科技攻关项目;江西省科技厅科技攻关项目 |
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| 摘 要： | 目的:测定彭泽贝母中微量元素含量,研究彭泽贝母中微量元素的存在形态,探讨微量元素的含量和形态.方法:采用HNO3-H2O2微波消解体系,电感耦合等离子质谱法(ICP-MS)测定彭泽贝母中铅、钙、铁、锰、锌、镉、钡、铬等10种微量元素的含量,初步探究微量元素的存在形态.结果:Ca元素在彭泽贝母中含量最高,而Mo元素含量最低;彭泽贝母中微量元素是以无机态为主、多种形态共存的复杂体系.结论:彭泽贝母中含有丰富的人体必需微量元素,可能促进其有效成分作用的发挥.
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| 关 键 词： | 彭泽贝母 ICP-MS法 微量元素 形态分析 |
| 文章编号： | 1006-3757（2006）04-0208-05 |
| 收稿时间： | 2006-07-17 |
| 修稿时间： | 2006-10-09 |
Determination and Speciation Analysis of Trace Elements in Fritillaria monantha Migo By ICP-MS |
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| ZHONG You-quan,YANG Jie,HAN Xiu-lin,CAO Lan and WAN Chun-hua.Determination and Speciation Analysis of Trace Elements in Fritillaria monantha Migo By ICP-MS[J].Analysis and Testing Technology and Instruments,2006,12(4):208-212. |
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| Authors: | ZHONG You-quan YANG Jie HAN Xiu-lin CAO Lan and WAN Chun-hua |
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| Institution: | Jiangxi University of Traditional Chinese Medicine, Nanchang 330006, China;Jiangxi University of Traditional Chinese Medicine, Nanchang 330006, China;Jiangxi University of Traditional Chinese Medicine, Nanchang 330006, China;Jiangxi University of Traditional Chinese Medicine, Nanchang 330006, China;Jiangxi Center of Analysis & Measurement, Nanchang 330029, China |
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| Abstract: | Objective:To determine the content and study on the speciation of the trace elements in Fritillaria monantha Migo.and discuss the relationship among the content & the speciation of the trace elements and efficancy of medicine.Methods: The content & the speciation of ten trace elements was determined by microwave-digestion with HNO_3-H_2O_2 and ICP-MS.Results: Among the ten trace elements,the content of Ca was the highest,and the lowest content was Mo;the trace elements are mainly formed in inorganic species and the others in Fritillaria monantha Migo which include various elements.Conclusion:The dosages of useful micro and trace elements within Fritillaria monantha Migo can makeup or adjust the functions of human being,these elements may increase the roles of efficient composition. |
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| Keywords: | Fritillaria monantha Migo ICP-MS trace element speciation analysis |
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