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Massenspektrometrie kondensierter N-Heterocyclen. 1–Elektronenstoßinduzierte Bildung von Cyclaziniumionen aus 5-Aryl(Hetaryl)-9-methyl-s-triazolo[4,3-c]tetrazolo-[1,5-a]pyrimidinen
Authors:Anderas K  nnecke,Peter Lepom,Ronald D  rre,Eberhard Lippmann
Affiliation:Anderas Könnecke,Peter Lepom,Ronald Dörre,Eberhard Lippmann
Abstract:The electron impact mass spectra of 5-aryl(hetaryl)-9-methyl-s-triazolo[4,3-c]tetrazolo[1,5- a]pyrimidines have been investigated. There is a general fragmentation mechanism, which forms stable cyclazinium ions by cyclization. In the case of the 5-hetaryl derivatives the proposed structures were confirmed by means of a comparison of mass analysed ion kinetic energy spectra with suitable model compounds.
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