Dodecylphosphonic acid (DPA): a highly efficient catalyst for the synthesis of 2H-indazolo[2,1-b]phthalazine-triones under solvent-free conditions |
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Authors: | Mazaahir Kidwai Anwar Jahan Ritika Chauhan Neeraj Kumar Mishra |
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Institution: | 1. Green Chemistry Research Laboratory, Department of Chemistry, University of Delhi, Delhi 110 007, India |
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Abstract: | A new green protocol has been developed for the synthesis of 2H-indazolo2,1-b]phthalazine-triones via one-pot, three-component condensation reaction of aromatic aldehydes with 1,3-dicarbonyl compounds and phthalhydrazide using reusable dodecylphosphonic acid (DPA) as heterogeneous solid acid catalyst under solvent-free conditions. This protocol provides a novel and improved method for obtaining 2H-indazolo2,1-b]phthalazine-triones in terms of good yields with little catalyst loading. |
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