| 3-甲基-9-芳基-1,8-二氧代-2,10-二氧杂蒽衍生物的合成 |
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| 引用本文： | 游新奎,林志兰,张雪利,高原. 3-甲基-9-芳基-1,8-二氧代-2,10-二氧杂蒽衍生物的合成[J]. 有机化学, 2012, 32(1): 156-159 |
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| 作者姓名： | 游新奎 林志兰 张雪利 高原 |
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| 作者单位： | 深圳大学化学与化工学院 深圳518060 |
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| 基金项目： | 国家自然科学基金，广东省自然科学基金 |
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| 摘 要： | 以芳醛、4-羟基-6-甲基-2-吡喃酮和1,3-环己二酮为原料,乙二醇为溶剂合成了一系列3-甲基-9-芳基-1,8-二氧代-2,10-二氧杂蒽衍生物.该反应产率高(70%～83%)、操作简单、后处理方便.产物的结构经红外光谱、核磁共振谱及单晶X射线衍射法表征.
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| 关 键 词： | 芳醛 4-羟基-6-甲基-2-吡喃酮 1,3-环己二酮 二氧杂蒽 晶体结构 |
Synthesis of 9-Aryl-3-methyl-1,8-dioxo-2,10-dioxanthens |
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| You,Xinkui , Lin,Zhilan , Zhang,Xueli , Gao,Yuan. Synthesis of 9-Aryl-3-methyl-1,8-dioxo-2,10-dioxanthens[J]. Chinese Journal of Organic Chemistry, 2012, 32(1): 156-159 |
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| Authors: | You Xinkui Lin Zhilan Zhang Xueli Gao Yuan |
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| Affiliation: | You,Xinkui Lin,Zhilan Zhang,Xueli Gao,Yuan(College of Chemistry and Chemical Engineering,Shenzhen University,Shenzhen 518060) |
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| Abstract: | A series of 9-aryl-3-methyl-1,8-dioxo-2,10-dioxanthens were synthesized by the reaction of aromatic aldehydes,4-hydroxyl-6-methyl-2-pyranone and 1,3-cyclohexadione in glycol.The structures of the products were determined by IR,NMR and X-ray diffraction analysis. |
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| Keywords: | aromatic aldehyde 4-hydroxyl-6-methyl-2-pyranone 1,3-cyclohexadione dioxanthen crystal stucture |
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