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N,N,N′,N′‐Tetraalkylaminoazoxybenzene Derivatives; Convenient Synthesis and Mechanistic Study
Authors:Long‐Li Lai  Yi‐Ging Chang  Hui‐Chu Hsu  Shun‐Ju Hsu  Dao‐Wen Luo
Affiliation:1. Department of Applied Chemistry, National Chi Nan University, Puli, Taiwan 545, R.O.C.;2. Instrumentation Center, National Chung‐Hsing University, Taichung, Taiwan 402, R.O.C.
Abstract:N,N,N′,N′‐tetraalkyaminoazoxybenzene derivatives were conveniently prepared by the coupling of N,N‐dialkylnitrosoaniline in the presence of acetone and KOH. The reaction mechanism was proposed and investigated, and the structure of compound 3b was also confirmed by single crystal X‐ray diffractometry.
Keywords:Azoxybenzene  Nitrosoaniline  N,N,N′  ,N′  ‐Tetraalkyaminoazoxybenzene
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