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Effect of lead doping in the system Bi-Sr-Ca-Cu-O on the formation of 2212 crystals, grown from a KCl flux using pre-synthesized compounds (precursors)
Authors:V N Osipov  I N Zimkin  V N Gurin  Yu G Nosov
Institution:(1) A. F. Ioffe Physicotechnical Institute, Russian Academy of Sciences, 194021 St. Petersburg, Russia
Abstract:A combination of the solution-melt method and solid-phase synthesis of complex oxides has been used to obtain crystals of Bi2Sr2CaCu2O8 (2212). Partial substitution of bismuth by lead leads to a change in the orientation of the growth layers in the (001) plane of the 2212 crystal which has an orthorhombic lattice. An increase in the dimensions is noted along with an enhancement of the quality of the crystals when lead is introduced into the composition of the precursors. Fiz. Tverd. Tela (St. Petersburg) 39, 219–221 (February 1997)
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