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Coulometric titrations of arsenic(III) and antimony(III) with electrically generated bromine in acetic acid
Authors:TJ Pastor  VJ Vajgand  VV Antonijević
Institution:Department of Chemistry, Faculty of Sciences, University of Belgrade Yugoslavia
Abstract:Conditions for the coulometric titrations were investigated. Arsenic(III) could be titrated by continuous or discontinuous generation of bromine, and antimony(III) by discontinuous generation or back-titration. The accuracy and reproducibility depend on the pretreatment of the platinum electrodes.
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