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新疆野生樱桃李及栽培品种果肉中17种元素含量ICP-MS法测定
引用本文:沈静,薛海燕,李改茹,鹿毅,姚军. 新疆野生樱桃李及栽培品种果肉中17种元素含量ICP-MS法测定[J]. 光谱学与光谱分析, 2014, 34(9): 2557-2560. DOI: 10.3964/j.issn.1000-0593(2014)09-2557-04
作者姓名:沈静  薛海燕  李改茹  鹿毅  姚军
作者单位:1. 新疆医科大学第五附属医院药剂科, 新疆 乌鲁木齐 830011
2. 新疆产品质量监督检验研究院,新疆 乌鲁木齐 830004
3. 新疆医科大学药学院,新疆 乌鲁木齐 830011
基金项目:The National Natural Science Foundation of China (31160322) and the Project of Scientific Research Innovation Fund of Xinjiang Medical University(XJC2012132)
摘    要:比较紫色,红色和黄色三种新疆野生樱桃李及栽培品种果肉中无机元素的含量,样品采用微波消解方法进行前处理,ICP-MS法检测其中K,Ca,Mg,Na,Fe,Mn,Cu,Zn,Be,Li,Se,Sr,Cr,Pb,Cd,As,Hg等17种元素。该检测方法快速简便,精密度高且具有较高的灵敏度,17种元素的加标回收率在93.5%~110.4%。分析结果表明紫色,红色和黄色三种新疆野生樱桃李及栽培品种果肉中的17种元素含量均较为接近,均含有极为丰富的K元素,含量高达1‰左右,Ca,Mg,Na,Fe,Mn均为含量较高的金属元素且含量依次降低,Cu,Zn,Li,Se,Sr,Cr也有一定含量,Pb,Cd,As,Hg等有害元素含量极低或未检出。实验结果为研究新疆野生樱桃李与栽培品种果肉中微量元素含量提供参考数据。

关 键 词:新疆野生樱桃李  栽培品种  元素分析  ICP-MS   
收稿时间:2013-12-23

Measuring the Content of 17 Elements in the Flesh of Prunus Cerasifera and Its Cultivars by ICP-MS
SHEN Jing;XUE Hai-yan;LI Gai-ru;LU Yi;YAO Jun. Measuring the Content of 17 Elements in the Flesh of Prunus Cerasifera and Its Cultivars by ICP-MS[J]. Spectroscopy and Spectral Analysis, 2014, 34(9): 2557-2560. DOI: 10.3964/j.issn.1000-0593(2014)09-2557-04
Authors:SHEN Jing  XUE Hai-yan  LI Gai-ru  LU Yi  YAO Jun
Affiliation:1. Department of Pharmacy, the Fifth Affiliated Hospital, Xinjiang Medical University, Urumqi 830011, China2. Xinjiang Supervision and Inspection Institute for Product Quality, Urumqi 830004, China3. College of Pharmacy, Xinjiang Medical University, Urumqi 830011, China
Abstract:The present study compared the contents of inorganic elements in the pulp of purple, red, and yellow Prunus cerasifera with its cultivars. A method was established for the analysis of 17 kinds of trace elements (K, Ca, Mg, Na, Fe, M n, Cu, Zn, Be, Li, Se, Sr, Cr, Pb, Cd, As and Hg) in the flesh of Prunus cerasifera by microwave digestion- ICP-MS. The detection method is simple and quick, yet shoes high precision and high sensitivity. The recovery rate of 17 elements ranged from 93.5% to 110.4%. The analysis results showed that the contents of 17 elements in the flesh of purple, red, and yellow Prunus cerasifera and its cultivars are similar, containing extremely rich K elements (as high as 1 ‰) and higher contents of Ca, Mg, Na, Fe and Mn. The contents of Cu, Zn, Li, Se, Sr and Cr are also present. The contents of Pb, Cd, As, Hg and other harmful element are either very low or not detectable. The experimental results for the study of trace elements in pulp of Prunus cerasifera and its cultivars provide empirical data for future research in this area.
Keywords:Prunus cerasifera  Cultivars  Elemental analysis  ICP-MS
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