Assay of d-cycloserine by chloramine-B,bromamine-T,and bromamine-B |
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| Authors: | B. Jayaram N.M. Made Gowda |
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| Affiliation: | Department of Chemistry, V.V. Pura College of Science, Bangalore-560 004 India;Division of Biochemistry, Department of Human Biological Chemistry & Genetics, The University of Texas Medical Branch, Galveston, TX, 77550 U.S.A. |
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| Abstract: | The reaction between d-cycloserine (DCS) and aromatic N-haloamines proceeds quantitatively over a wide range of experimental conditions. Simple titrimetric procedures for the assay of DCS are described. Oxidation of DCS involves an eight-electron change and the oxidation products are identified. The methods can be used for the assay of the antibiotic in medicinal preparations as well as for calculating the number of ligand molecules present in metal complexes of DCS. |
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