Assigning the configuration of amino alcohols by NMR: a single derivatization method |
| |
| Authors: | Leiro Victoria Seco José Manuel Quiñoá Emilio Riguera Ricardo |
| |
| Affiliation: | Departamento de Química Orgánica, Facultad de Química y Unidad de RMN de Biomoléculas Asociada al CSIC, Universidad de Santiago de Compostela, E-15782 Santiago de Compostela, Spain. |
| |
| Abstract: | The chirality of sec/prim- and prim/sec-1,2-amino alcohols can be determined by (1)H NMR of just one MPA derivative--either (R) or (S)--by comparison of two spectra at different temperatures and analysis of the evolution of the easily observable singles of the CalphaH signals. |
| |
| Keywords: | |
| 本文献已被 PubMed 等数据库收录！ |
|
